Journal article
Microwave-Assisted Solvent-Free Synthesis of Zeolitic Imidazolate Framework-67
Journal of nanomaterials, Vol.2016, pp.1-9
2016
Handle:
https://hdl.handle.net/2376/114265
Abstract
A microporous metal-organic framework (MOF), cobalt-based zeolitic imidazolate framework-67 (ZIF-67), was synthesized by the combination of solvent-free hand-mill and microwave irradiation, without any organic solvent and within 30 minutes. The hand-milling process can mix the reactants well by the virtue of high moisture/water absorption capacity of reactants. In addition, the outstanding electromagnetic wave absorption capability of cobalt leads to efficient conversion to MOF structures before carbonization. The obtained ZIF-67 possesses high surface area and micropore volume.
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Details
- Title
- Microwave-Assisted Solvent-Free Synthesis of Zeolitic Imidazolate Framework-67
- Creators
- Heng Zhang - Key Laboratory of Structure Dynamic Behavior and Control (Harbin Institute of Technology), Ministry of Education, Harbin, Heilongjiang 150090, China, School of Civil Engineering, Harbin Institute of Technology, Harbin 150090, China, School of Civil Engineering and Architecture, Wuhan Polytechnic University, Wuhan 430023, ChinaJing Zhong - Key Laboratory of Structure Dynamic Behavior and Control (Harbin Institute of Technology), Ministry of Education, Harbin, Heilongjiang 150090, China, School of Civil Engineering, Harbin Institute of Technology, Harbin 150090, China, School of Civil Engineering and Architecture, Wuhan Polytechnic University, Wuhan 430023, ChinaGuoxiang Zhou - School of Civil Engineering and Architecture, Wuhan Polytechnic University, Wuhan 430023, ChinaJunliang Wu - School of Civil Engineering and Architecture, Wuhan Polytechnic University, Wuhan 430023, ChinaZhenyu Yang - Department of Chemistry, Nanchang University, Nanchang 330031, ChinaXianming Shi - Department of Civil & Environmental Engineering, Washington State University, P.O. Box 642910, Pullman, WA 99164-2910, USA
- Publication Details
- Journal of nanomaterials, Vol.2016, pp.1-9
- Academic Unit
- Civil and Environmental Engineering, Department of
- Identifiers
- 99900548014901842
- Language
- English
- Resource Type
- Journal article